[IrCl₄(2-(phenylazo)pyridine)]Cl

Base Information

• Chemical Name: [IrCl₄(2-(phenylazo)pyridine)]Cl
• CAS No.: 777855-58-0
• Molecular Formula: C₁₁H₉Cl₄IrN₃*Cl
• Molecular Weight: 552.698
• Mol file: 777855-58-0.mol

Synonyms:

Chemical Property of [IrCl₄(2-(phenylazo)pyridine)]Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [IrCl₄(2-(phenylazo)pyridine)]Cl

There total 1 articles about [IrCl₄(2-(phenylazo)pyridine)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-(phenylazo)pyridine (2569-57-5) + iridium(III) chloride trihydrate → (IrCl2(NC5H4NNC6H5)(NC5H4NNC6H4)) (777855-57-9) + [IrCl4(2-(phenylazo)pyridine)]Cl (777855-58-0)

Guidance literature:

In methanol; IrCl3*3H2O and 2-(phenylazo)pyridine in MeOH were refluxed on steam bathfor 4 h; soln. was filtered, filtrate was evapd. to dryness, residue was extd. with CH2Cl2; elem. anal.;

DOI:10.1039/b407209j

Reference yield:

[IrCl4(2-(phenylazo)pyridine)]Cl (777855-58-0) + sodium perchlorate → [IrCl4(2-(phenylazo)pyridine)]ClO4

Guidance literature:

In water; acetonitrile; aq. soln. NaClO4 was added to soln. Ir complex in MeCN;

DOI:10.1039/b407209j

upstream raw materials:

2-(phenylazo)pyridine