dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

Base Information

Chemical Name:dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan
CAS No.:115505-14-1
Molecular Formula:C₁₇H₃₃OP
Molecular Weight:284.422
Hs Code.:

Synonyms:

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Chemical Property of dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

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Technology Process of dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

There total 1 articles about dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13830-12-1
2-(2-chloroethoxy)propane

: 829-84-5
dicyclohexylphosphane

: 115505-14-1
dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, THF, 0 deg C than 20 deg C, 0.5 h 2.) reflux, 15 min;
DOI:10.1016/0022-328X(87)85173-2

Reference yield: 66.0%

: 14040-11-0
tungsten hexacarbonyl

: 115505-14-1
dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

: 115557-48-7
pentacarbonyl{dicyclohexyl{2-(1-methylethoxy)ethyl}phosphine}tungsten

Guidance literature:: With THF; In tetrahydrofuran; Irradiation (UV/VIS); a soln. of W(CO)6 in THF was irradiated at 20°C under inert atmosphere with Hg-lamp for 2 h with stirring, THF soln. of a small excess of the phosphine was added dropwise within 0.5 h, mixt. was stirred at room temp. for 5 h; solvent was evapd. under high vac., residue was digested in pentane, filtered, cooled to -30°C, crystals were collected, unreacted W(CO)6 was removed by sublimation; elem. anal.;
DOI:10.1016/0022-328X(87)85173-2

Reference yield:

: 115505-14-1
dicyclohexyl<2-(1-methylethoxy)ethyl>phosphan

: 115557-51-2
tetracarbonyl{dicyclohexyl{2-(1-methylethoxy)ethyl}phosphine-O,P}tungsten

Guidance literature:: Multi-step reaction with 2 steps

1: THF / tetrahydrofuran

2: not given

With THF; In tetrahydrofuran;
DOI:10.1016/0022-328X(87)85173-2