N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

Base Information

Chemical Name:N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide
CAS No.:1310404-39-7
Molecular Formula:C₄₇H₇₆N₄O₆
Molecular Weight:793.144
Hs Code.:

Synonyms:

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Chemical Property of N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

Chemical Property:

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Technology Process of N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

There total 6 articles about N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1310404-38-6
N-(2-nitrobenzyl)-11-aminoundecanol

: 1310404-36-4
3,5-bis-((3S)-3,7-dimethyloctylaminocarbonyl)benzoic acid chloride

: 1310404-39-7
N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

Guidance literature:: N-(2-nitrobenzyl)-11-aminoundecanol; With potassium carbonate; In chloroform; Inert atmosphere;

3,5-bis-((3S)-3,7-dimethyloctylaminocarbonyl)benzoic acid chloride; In chloroform; at 20 ℃; Cooling with ice; Inert atmosphere;
DOI:10.1002/anie.201100104

Reference yield:

: 1310404-37-5
N-(2-nitrobenzylidene)-11-aminoundecanol

: 1310404-39-7
N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

2.1: potassium carbonate / chloroform / Inert atmosphere

2.2: 20 °C / Cooling with ice; Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; In ethanol; chloroform;
DOI:10.1002/anie.201100104

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1310404-39-7
N,N'-bis-((3S)-3,7-dimethyloctyl)-N''-(11-hydroxyundecyl)-N''-(2-nitrobenzyl)benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / Inert atmosphere; Heating

2.1: hydrazine / tetrahydrofuran; water / 18 h / Reflux; Inert atmosphere

3.1: ethanol / Reflux; Inert atmosphere

4.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

5.1: potassium carbonate / chloroform / Inert atmosphere

5.2: 20 °C / Cooling with ice; Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; hydrazine; In tetrahydrofuran; ethanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201100104