N-benzyloxycarbonyl-α-L-mycosamine

Base Information

Chemical Name:N-benzyloxycarbonyl-α-L-mycosamine
CAS No.:1392477-03-0
Molecular Formula:C₁₄H₁₉NO₆
Molecular Weight:297.308
Hs Code.:

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Chemical Property of N-benzyloxycarbonyl-α-L-mycosamine

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-α-L-mycosamine

There total 7 articles about N-benzyloxycarbonyl-α-L-mycosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₇NO₆Si

: 1392477-03-0
N-benzyloxycarbonyl-α-L-mycosamine

: 1392477-05-2
N-benzyloxycarbonyl-β-L-mycosamine

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 20 ℃; for 2.5h; optical yield given as %de;
DOI:10.1039/c2ob25793a

Reference yield:

: C₁₄H₂₇N₃O₃Si

: 1392477-03-0
N-benzyloxycarbonyl-α-L-mycosamine

: 1392477-05-2
N-benzyloxycarbonyl-β-L-mycosamine

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / -35 - -20 °C / Inert atmosphere

2: pyridinium p-toluenesulfonate / dichloromethane / 20 °C / Inert atmosphere

3: water; trimethylphosphane / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / methanol / 1.58 h / 0 - 20 °C / Inert atmosphere

5: 2,6-dimethylpyridine; sodium periodate; potassium osmate(VI) dihydrate / 1,4-dioxane; water / 2 h / 20 °C

6: hydrogen fluoride / acetonitrile / 2.5 h / 20 °C

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; hydrogen fluoride; water; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; acetic acid; tetramethylammonium triacetoxyborohydride; trimethylphosphane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; 3: Staudinger reaction;
DOI:10.1039/c2ob25793a

Reference yield:

: 1392476-91-3
(2S,3R,4S,5S,6E)-4-azido-2-tert-butyldimethylsilyloxy-6-octene-3,5-diol

: 1392477-03-0
N-benzyloxycarbonyl-α-L-mycosamine

: 1392477-05-2
N-benzyloxycarbonyl-β-L-mycosamine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C / Inert atmosphere

2: water; trimethylphosphane / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

3: sodium hydrogencarbonate / methanol / 1.58 h / 0 - 20 °C / Inert atmosphere

4: 2,6-dimethylpyridine; sodium periodate; potassium osmate(VI) dihydrate / 1,4-dioxane; water / 2 h / 20 °C

5: hydrogen fluoride / acetonitrile / 2.5 h / 20 °C

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; hydrogen fluoride; water; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; trimethylphosphane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; 2: Staudinger reaction;
DOI:10.1039/c2ob25793a