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Technology Process of (CO)3CrC6H4(CHO)C6H5

(CO)3CrC6H4(CHO)C6H5

Base Information
  • Chemical Name:(CO)3CrC6H4(CHO)C6H5
  • CAS No.:197316-13-5
  • Molecular Formula:C16H10CrO4
  • Molecular Weight:318.249
  • Hs Code.:
(CO)3CrC<sub>6</sub>H<sub>4</sub>(CHO)C<sub>6</sub>H<sub>5</sub>

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Chemical Property of (CO)3CrC6H4(CHO)C6H5
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Technology Process of (CO)3CrC6H4(CHO)C6H5

There total 2 articles about (CO)3CrC6H4(CHO)C6H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(CO)3CrC<sub>6</sub>H<sub>5</sub>CHNC<sub>6</sub>H<sub>11</sub>

(CO)3CrC6H5CHNC6H11

phenyllithium
591-51-5

phenyllithium

(CO)3CrC<sub>6</sub>H<sub>4</sub>(CHO)C<sub>6</sub>H<sub>5</sub>
146987-40-8,197316-13-5,146931-31-9

(CO)3CrC6H4(CHO)C6H5

Guidance literature:
With {Ph3C}{BF4}; In tetrahydrofuran; addn. of PhLi to Cr-complex soln. (inert atmosphere) according to E.P.Kuendig, D.Amurrio, R.Liu, A.Ripa, Synlett 1991, 2, 657, evapn., dissolution in CH2Cl2 at room temp., addn. of Ph3CBF4 in CH2Cl2, stirring overnight; aq. workup, column chromy. (silica gel);
DOI:10.1002/hlca.19920750818

Reference yield: 55.0%

(CO)3CrC<sub>6</sub>H<sub>5</sub>CHNC<sub>4</sub>NH<sub>7</sub>CH<sub>2</sub>OCH<sub>3</sub>

(CO)3CrC6H5CHNC4NH7CH2OCH3

phenyllithium
591-51-5

phenyllithium

(CO)3CrC<sub>6</sub>H<sub>4</sub>(CHO)C<sub>6</sub>H<sub>5</sub>
197316-13-5,146987-40-8,146931-31-9

(CO)3CrC6H4(CHO)C6H5

Guidance literature:
With {Ph3C}{BF4}; In tetrahydrofuran; byproducts: (R)-phenyl-complex; react. of Cr-complex with PhLi at -78 to -40°C for 6 h, evapn., react. with Ph3CBF4 in CH2Cl2 at room temp. overnight, hydrolysis with 50% aq. H2SO4 in MeOH at 40°C for 48 h;
DOI:10.1002/hlca.19920750818
upstream raw materials:

phenyllithium

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