Technology Process of C36H43F3N6O2Si
There total 8 articles about C36H43F3N6O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 - 80 ℃;
Sealed tube;
Inert atmosphere;
DOI:10.1021/jm301581y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 - 60 °C / Inert atmosphere
2: potassium carbonate; methanol / 20 °C / Inert atmosphere
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 80 °C / Sealed tube; Inert atmosphere
With
methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide; acetonitrile;
1: |Sonogashira Cross-Coupling / 3: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301581y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran / 3 h / -20 - 20 °C / Inert atmosphere
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 - 60 °C / Inert atmosphere
3: potassium carbonate; methanol / 20 °C / Inert atmosphere
4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 80 °C / Sealed tube; Inert atmosphere
With
methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301581y