(1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

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Chemical Name:(1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester
CAS No.:898262-99-2
Molecular Formula:C₃₂H₃₂BrF₁₇N₂O₄
Molecular Weight:911.494
Hs Code.:

(1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

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Chemical Property of (1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

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Technology Process of (1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

There total 1 articles about (1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Amino-4-methyl-pentanoic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

: 4144-22-3
N-tert-butylmaleimide

: 1122-91-4
4-bromo-benzaldehyde

: 898262-99-2
(1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 130 ℃; for 0.333333h; microwave irradiation;
DOI:10.1002/ejoc.200600077

Reference yield:

: 898262-99-2
(1R,3S,3aR,6aS)-3-(4-Bromo-phenyl)-5-tert-butyl-1-isobutyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

: (5S,5aR,8aS,8bR)-5-(4-Bromo-phenyl)-7-tert-butyl-2-(3-chloro-phenyl)-8b-isobutyl-tetrahydro-pyrrolo[3',4':3,4]pyrrolo[1,2-c]imidazole-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-4-dimethylaminopyridine / toluene / 0.17 h / 130 °C / microwave irradiation

2: 75 percent / K₂CO₃ / dimethylformamide / 0.08 h / 120 °C / microwave irradiation

With potassium carbonate; dmap; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.200600077