C₃₃H₄₀N₂O₄STe

Base Information

Chemical Name:C₃₃H₄₀N₂O₄STe
CAS No.:1430324-64-3
Molecular Formula:C₃₃H₄₀N₂O₄STe
Molecular Weight:688.358
Hs Code.:

C<sub>33</sub>H<sub>40</sub>N<sub>2</sub>O<sub>4</sub>STe

Synonyms:

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Chemical Property of C₃₃H₄₀N₂O₄STe

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Technology Process of C₃₃H₄₀N₂O₄STe

There total 7 articles about C₃₃H₄₀N₂O₄STe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189110-55-1
4-(tert-butylthio)but-2-ynal

: C₂₅H₂₈N₂O₄Te

: 1430324-64-3
C₃₃H₄₀N₂O₄STe

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1021/ja402933s

Reference yield:

: 1430324-60-9
tert-butyl 2-(5-methoxy-1-methyl-2-vinyl-1H-indol-3-yl)ethylcarbamate

: 1430324-64-3
C₃₃H₄₀N₂O₄STe

Guidance literature:: Multi-step reaction with 5 steps

1.1: (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate / acetonitrile / 0.08 h / -20 °C

1.2: 6 h / -20 °C

2.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; water / tetrahydrofuran; tert-butyl alcohol / 1.33 h / 0 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.67 h

3.2: 0.33 h

4.1: trifluoroacetic acid / 0.03 h / 20 °C

5.1: sodium tris(acetoxy)borohydride / dichloromethane / 0.08 h / 20 °C

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogen phosphate monohydrate; (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate; water; sodium tris(acetoxy)borohydride; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja402933s

Reference yield:

: 380358-27-0
3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole

: 1430324-64-3
C₃₃H₄₀N₂O₄STe

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

1.2: 0.5 h / 0 °C

2.1: n-butyllithium / 1,2-dimethoxyethane / 3 h / -78 - -40 °C / Schlenk technique; Inert atmosphere

2.2: 1.5 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

2.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere

3.1: (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate / acetonitrile / 0.08 h / -20 °C

3.2: 6 h / -20 °C

4.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; water / tetrahydrofuran; tert-butyl alcohol / 1.33 h / 0 °C

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.67 h

5.2: 0.33 h

6.1: trifluoroacetic acid / 0.03 h / 20 °C

7.1: sodium tris(acetoxy)borohydride / dichloromethane / 0.08 h / 20 °C

With sodium chlorite; sodium tetrahydroborate; n-butyllithium; sodium dihydrogen phosphate monohydrate; (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate; water; sodium tris(acetoxy)borohydride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol;
DOI:10.1021/ja402933s