[1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate

Base Information

Chemical Name:[1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate
CAS No.:164987-07-9
Molecular Formula:BF₄*C₂₉H₃₂OP₂SW*F₆P
Molecular Weight:906.205
Hs Code.:

[1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate

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Chemical Property of [1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate

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Technology Process of [1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate

There total 1 articles about [1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: carbonyl-(η5-cyclopentadienyl)(trimethylphosphine){η2-(diphenylphosphino)phenylcarbene}tungsten hexafluorophosphate

: 5799-67-7
dimethyl(methylthio)sulfonium tetrafluoroborate

: 164987-07-9
[1-carbonyl-1-(η(5)-cyclopentadienyl)-4-methyl-2,2,3-triphenyl-1-trimethylphosphine-1-tungsta-2-phospha-4-thia-bicyclo[1.1.0]butane] tetrafluoroborate/hexafluorophosphate

Guidance literature:: In dichloromethane; N2-atmosphere; addn. of 1 equiv. sulfonium salt to W-complex at -78°C, stirring at room temp. for 24 h (pptn.); collection (filtration), washing (CH2Cl2), pptn. from MeCN/CH2Cl2/ether/pentane, drying (vac.); elem. anal.;
DOI:10.1016/0022-328X(94)05246-8