cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

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Chemical Name:cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane
CAS No.:148843-47-4
Molecular Formula:C₇₂H₁₄₀S₃Si₁₂Sn₂
Molecular Weight:1676.55
Hs Code.:

Synonyms:

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Chemical Property of cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

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Technology Process of cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

There total 1 articles about cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 135139-71-8
(mesityl)(2,4,6-tris{bis(trimethylsilyl)methyl}phenyl)SnS₄

: 148843-47-4,148843-46-3
cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

: trans-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

Guidance literature:: With HMPT; In tetrahydrofuran; addn. of HMPT to the stannolane in THF at room temp., stirred at room temp. for 10 h under Ar; evapd., chromy., recrystn. (ethanol/CHCl3), elem. anal.;
DOI:10.1021/om00031a030

Reference yield: 69.0%

: 148843-47-4,148843-46-3
cis-3,5-dimesityl-3,5-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,2,4,3,5-trithiadistannolane

: 143953-68-8,147424-57-5
cis-2,4-dimesityl-2,4-bis{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}-1,3,2,4-dithiadistannetane

Guidance literature:: With HMPT; In benzene; Irradiation (UV/VIS); the thiastannolane and HMPT in C6H6 is irradiated by a high-pressure Hg lamp for 1,5 h under ice cooling and Ar; evapd., chromy.;
DOI:10.1021/om00031a030