trans-(meso-tetra-p-tolylporphyrinato)SnMeBr

Base Information

• Chemical Name: trans-(meso-tetra-p-tolylporphyrinato)SnMeBr
• CAS No.: 209852-99-3
• Molecular Formula: C₄₉H₃₉BrN₄Sn
• Molecular Weight: 882.489

Synonyms:

Chemical Property of trans-(meso-tetra-p-tolylporphyrinato)SnMeBr

Chemical Property:

Purity/Quality:

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Technology Process of trans-(meso-tetra-p-tolylporphyrinato)SnMeBr

There total 1 articles about trans-(meso-tetra-p-tolylporphyrinato)SnMeBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

5,10,15,20-tetra-p-tolylporphyrin, dilithium salt * 2 THF + dimethyltin dibromide (2767-47-7) → trans-(meso-tetra-p-tolylporphyrinato)SnMeBr (209852-99-3)

Guidance literature:

In dichloromethane; inert atmosphere, in dark; addn. of 1 equiv. Me2SnBr2 to Li-compd. at -34°C, standing at -34°C for 23 h; filtration, concn., layering with Et2O, crystn. (-34°C), collection (filtration), washing (Et2O), drying (vac.); elem. anal.;

upstream raw materials:

dimethyltin dibromide

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