OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

Base Information

Chemical Name:OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)
CAS No.:915200-87-2
Molecular Formula:C₆₆H₅₄ClNO₃P₂W
Molecular Weight:1190.41
Hs Code.:

OHCHNC<sub>6</sub>H<sub>2</sub>(CH(CH<sub>3</sub>)2)2C<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CW(CO)2Cl(P<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)4CH<sub>2</sub>CH<sub>2</sub>)

Synonyms:

Suppliers and Price of OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

There total 1 articles about OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 211446-84-3
W(CO)2Cl(dppe)(CC₆H₄I)

: 915200-85-0
OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂H

: 915200-87-2
OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

Guidance literature:: With cis-PdCl₂(P(C₆H₅)3)2; CuI; diethylamine; In tetrahydrofuran; (under inert atm.); W-complex dissolved in THF, diethylamine added, ligand, cis-PdCl2(P(C6H5)3)2 and CuI added, stirred at room temp. overnight; solvent removed in vacuo, residue washed with hexane, dried, redissolvedin CH2Cl2, filtered, hexane added;
DOI:10.1016/j.jorganchem.2006.02.029

Reference yield: 46.0%

: 915200-87-2
OHCHNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

: 915200-88-3
CNC₆H₂(CH(CH₃)2)2C₂C₆H₄C₂C₆H₄C₂C₆H₄CW(CO)2Cl(P₂(C₆H₅)4CH₂CH₂)

Guidance literature:: With triethylamine; thiophosgene; In dichloromethane; (under inert atm.); W-complex dissolved in CH2Cl2, triethylamine added, cooled to -78°C, soln. of thiophosgene in CH2Cl2 added, warmed to0°C, stirred for 30 min; solvent removed in vacuo, residue washed with hexane, redissolved in THF, filtered, solvent removed in vacuo, redissolved in CH2Cl2, filtered, hexane added;
DOI:10.1016/j.jorganchem.2006.02.029