C₁₀H₁₈O

Base Information

• Chemical Name: C₁₀H₁₈O
• CAS No.: 1330048-77-5
• Molecular Formula: C₁₀H₁₈O
• Molecular Weight: 154.252
• Mol file: 1330048-77-5.mol

Synonyms:

Chemical Property of C₁₀H₁₈O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₈O

There total 5 articles about C₁₀H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H22O3 (1345866-27-4) → (R)-5-methyl-2-(prop-1-en-2-yl)hex-4-en-1-ol (498-16-8,21090-68-6) + C10H18O (1330048-77-5)

Guidance literature:

C₁₂H₂₂O₃; With thionyl chloride; triethylamine; at 25 ℃; for 3h;

With sodium hydroxide; In methanol; water;

DOI:10.1016/j.tetlet.2011.06.072

Reference yield:

(5S)-5-isopropenyl-2-methyl-octane-2,7-diol (1327155-05-4) → (R)-5-methyl-2-(prop-1-en-2-yl)hex-4-en-1-ol (498-16-8,21090-68-6) + C10H18O (1330048-77-5)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridinium chlorochromate / dichloromethane

2: Acremonium roseum AM₃₄₆ / water; acetone / 264 h / Enzymatic reaction

3: pyridine / 16 h / 8 °C

4: thionyl chloride; triethylamine / 3 h / 25 °C

With pyridine; thionyl chloride; triethylamine; pyridinium chlorochromate; In dichloromethane; water; acetone; 2: Baeyer-Villiger oxidation;

DOI:10.1016/j.tetlet.2011.06.072

Reference yield:

C12H22O2 (1327155-06-5) → (R)-5-methyl-2-(prop-1-en-2-yl)hex-4-en-1-ol (498-16-8,21090-68-6) + C10H18O (1330048-77-5)

Guidance literature:

Multi-step reaction with 3 steps

1: Acremonium roseum AM₃₄₆ / water; acetone / 264 h / Enzymatic reaction

2: pyridine / 16 h / 8 °C

3: thionyl chloride; triethylamine / 3 h / 25 °C

With pyridine; thionyl chloride; triethylamine; In water; acetone; 1: Baeyer-Villiger oxidation;

DOI:10.1016/j.tetlet.2011.06.072

upstream raw materials:

(R)-2-isopropenyl-5-methyl-hexane-1,5-diol

C₁₂H₂₂O₃

(5S)-5-isopropenyl-2-methyl-octane-2,7-diol

C₁₂H₂₂O₂