C₂₂H₂₁N₃O₅

Base Information

Chemical Name:C₂₂H₂₁N₃O₅
CAS No.:1258974-36-5
Molecular Formula:C₂₂H₂₁N₃O₅
Molecular Weight:407.426
Hs Code.:

C<sub>22</sub>H<sub>21</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₁N₃O₅

Chemical Property:

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Technology Process of C₂₂H₂₁N₃O₅

There total 11 articles about C₂₂H₂₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1258974-70-7
C₃₁H₄₁N₃O₅Si

: 1258974-36-5
C₂₂H₂₁N₃O₅

Guidance literature:: Inert atmosphere;
DOI:10.1021/jm1011269

Reference yield:

: 908567-28-2
C₁₁H₁₁BrO₃

: 1258974-36-5
C₂₂H₂₁N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate; ethanol / 40 °C

1.2: 80 °C

1.3: 20 °C

2.1: trifluorormethanesulfonic acid / dichloromethane / 15 h / 0 - 20 °C

2.2: 2 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 70 °C / Inert atmosphere

4.1: toluene / 0.5 h / 20 °C

5.1: pyridine; hydrogen fluoride / tetrahydrofuran

With pyridine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ethanol; trifluorormethanesulfonic acid; hydrogen fluoride; sodium carbonate; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 3.1: Suzuki coupling / 4.1: Aza-Diels-Alder reaction;
DOI:10.1021/co2001907

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 1258974-36-5
C₂₂H₂₁N₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyrrolidine / ethanol / Reflux

2.1: copper(ll) bromide / methanol; chloroform; ethyl acetate / Reflux

2.2: 20 °C

3.1: sodium tetrahydroborate; ethanol / 40 °C

3.2: 80 °C

3.3: 20 °C

4.1: trifluorormethanesulfonic acid / dichloromethane / 15 h / 0 - 20 °C

4.2: 2 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 70 °C / Inert atmosphere

6.1: toluene / 0.5 h / 20 °C

7.1: pyridine; hydrogen fluoride / tetrahydrofuran

With pyrrolidine; pyridine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ethanol; trifluorormethanesulfonic acid; hydrogen fluoride; sodium carbonate; copper(ll) bromide; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; ethyl acetate; toluene; 5.1: Suzuki coupling / 6.1: Aza-Diels-Alder reaction;
DOI:10.1021/co2001907