triphenylmethylgermatrane

Base Information

Chemical Name:triphenylmethylgermatrane
CAS No.:88076-37-3
Molecular Formula:C₂₅H₂₇GeNO₃
Molecular Weight:462.084
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylmethylgermatrane

Chemical Property:

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Technology Process of triphenylmethylgermatrane

There total 4 articles about triphenylmethylgermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 67453-19-4
germatrane

: 76-83-5
trityl chloride

: 70559-34-1
1-chlorogermatrane

: 88076-37-3
triphenylmethylgermatrane

: 519-73-3
triphenylmethane

Guidance literature:: In acetonitrile; byproducts: triethanolamine hydrobromide; under dry N2; mixt. boiled (81°C, 3 h); hot soln. decanted vac.-evapd. (20-100 mm, 30-35°C) until crystn. set in; ether added; solid 1-(triphenylmethyl)germatrane isolated; ppt. of chlorogermatrane obtained by evapn. of filtrate (40-50°C, 40mm); Ph3CH isolated from soln.; PMR;

Reference yield: 39.0%

: 88102-98-1
(C₆H₅)3CGe(OCH₂CH₃)3

: 88076-37-3
triphenylmethylgermatrane

Guidance literature:: With triethanolamine; In N,N-dimethyl-formamide; benzene; byproducts: ethanol; under dry N2; mixt. boiled for 3 h with removal of azeotropic mixt of benzene and ethanol; ppt. isolated on cooling; recrystd. from pentane;

Reference yield: 25.0%

: 67453-19-4
germatrane

: 88076-37-3
triphenylmethylgermatrane

Guidance literature:: With chloroform; In chloroform; under dry N2; mixt. boiled (1.3 mole % of galvinoxyl calcd. on germatrane taken, 61°C, 7 h); cooled; solid ppt. of germatranes filtered off; washed (ether); vac.-dried; notisolated, detected by PMR;