C₄₅H₆₈F₂N₄O₁₀

Base Information

Chemical Name:C₄₅H₆₈F₂N₄O₁₀
CAS No.:1357143-85-1
Molecular Formula:C₄₅H₆₈F₂N₄O₁₀
Molecular Weight:863.053
Hs Code.:

C<sub>45</sub>H<sub>68</sub>F<sub>2</sub>N<sub>4</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₄₅H₆₈F₂N₄O₁₀

Chemical Property:

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Technology Process of C₄₅H₆₈F₂N₄O₁₀

There total 7 articles about C₄₅H₆₈F₂N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271774-61-8
C₂₀H₃₁F₂N₃O₃

: 1357143-85-1
C₄₅H₆₈F₂N₄O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 18 h

3.1: sodium iodide; sodium hydride / tetrahydrofuran; mineral oil / 19 h / 0 - 20 °C

4.1: water; lithium hydroxide monohydrate / methanol / 20 °C

5.1: triethylamine / dmap / dichloromethane

With lithium hydroxide monohydrate; water; hydrogen; sodium hydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; dmap; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; mineral oil;

Reference yield:

: C₁₇H₂₅NO₄

: 1357143-85-1
C₄₅H₆₈F₂N₄O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dmap / tetrahydrofuran / 0 - 20 °C

2.1: sodium periodate / rhodium(III) chloride hydrate / ethyl acetate; acetonitrile; water / 18 h / 20 °C

3.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

3.2: 18 h / 0 - 20 °C

4.1: hydrogen / palladium on activated charcoal / methanol / 18 h

5.1: sodium iodide; sodium hydride / tetrahydrofuran; mineral oil / 19 h / 0 - 20 °C

6.1: water; lithium hydroxide monohydrate / methanol / 20 °C

7.1: triethylamine / dmap / dichloromethane

With pyridine; sodium periodate; lithium hydroxide monohydrate; water; hydrogen; sodium hydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; dmap; rhodium(III) chloride hydrate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; mineral oil;

Reference yield:

: 1357067-26-5
C₁₉H₂₇NO₅

: 1357143-85-1
C₄₅H₆₈F₂N₄O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium periodate / rhodium(III) chloride hydrate / ethyl acetate; acetonitrile; water / 18 h / 20 °C

2.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

2.2: 18 h / 0 - 20 °C

3.1: hydrogen / palladium on activated charcoal / methanol / 18 h

4.1: sodium iodide; sodium hydride / tetrahydrofuran; mineral oil / 19 h / 0 - 20 °C

5.1: water; lithium hydroxide monohydrate / methanol / 20 °C

6.1: triethylamine / dmap / dichloromethane

With sodium periodate; lithium hydroxide monohydrate; water; hydrogen; sodium hydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; dmap; rhodium(III) chloride hydrate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; mineral oil;