C₃₈H₆₁NO₈Si

Base Information

Chemical Name:C₃₈H₆₁NO₈Si
CAS No.:1429226-44-7
Molecular Formula:C₃₈H₆₁NO₈Si
Molecular Weight:687.99
Hs Code.:

C<sub>38</sub>H<sub>61</sub>NO<sub>8</sub>Si

Synonyms:

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Chemical Property of C₃₈H₆₁NO₈Si

Chemical Property:

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Technology Process of C₃₈H₆₁NO₈Si

There total 10 articles about C₃₈H₆₁NO₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-20-9
acetic acid methyl ester

: 1429226-42-5
C₃₅H₅₅NO₆Si

: 1429226-44-7
C₃₈H₆₁NO₈Si

: 1429226-43-6
C₃₈H₆₁NO₈Si

Guidance literature:: acetic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

C₃₅H₅₅NO₆Si; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Optical yield = 28.571 %de;
DOI:10.1016/j.tetlet.2013.01.110

Reference yield:

: C₂₈H₄₁NO₅

: 1429226-44-7
C₃₈H₆₁NO₈Si

: 1429226-43-6
C₃₈H₆₁NO₈Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C

2.1: 1H-imidazole / dichloromethane / 1 h / 0 °C

3.1: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C

4.1: Dess-Martin periodane; pyridine / dichloromethane / 3.5 h / 0 °C

5.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -78 °C

5.2: 2 h / -78 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; Dess-Martin periodane; triethylamine; calcium chloride; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110

Reference yield:

: 1429226-34-5
C₁₇H₂₇NO₄

: 1429226-44-7
C₃₈H₆₁NO₈Si

: 1429226-43-6
C₃₈H₆₁NO₈Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

2.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

3.1: copper(II) sulfate / dichloromethane / 18 h / 20 °C

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 3 h / -78 °C

4.2: 60 h / -60 °C

5.1: hydrogenchloride / water; 1,4-dioxane; methanol / 1 h / 20 °C

6.1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C

7.1: 1H-imidazole / dichloromethane / 1 h / 0 °C

8.1: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C

9.1: Dess-Martin periodane; pyridine / dichloromethane / 3.5 h / 0 °C

10.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -78 °C

10.2: 2 h / -78 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; diisobutylaluminium hydride; Dess-Martin periodane; copper(II) sulfate; triethylamine; calcium chloride; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110