C₅₂H₆₅N₇O₁₁S

Base Information

Chemical Name:C₅₂H₆₅N₇O₁₁S
CAS No.:1415034-23-9
Molecular Formula:C₅₂H₆₅N₇O₁₁S
Molecular Weight:996.194
Hs Code.:

C<sub>52</sub>H<sub>65</sub>N<sub>7</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₅₂H₆₅N₇O₁₁S

Chemical Property:

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Technology Process of C₅₂H₆₅N₇O₁₁S

There total 12 articles about C₅₂H₆₅N₇O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415034-26-2
C₅₃H₆₇N₇O₁₁S

: 1415034-23-9
C₅₂H₆₅N₇O₁₁S

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 0 ℃;
DOI:10.1021/jm301630s

Reference yield:

: 1415033-98-5
C₁₈H₂₀N₂O₅S

: 1415034-23-9
C₅₂H₆₅N₇O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C / Cooling with ice

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

5: water; lithium hydroxide / tetrahydrofuran; methanol / 0 °C

With 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm301630s

Reference yield:

: 5-methanesulfonylamino-isophthalic acid monomethyl ester

: 1415034-23-9
C₅₂H₆₅N₇O₁₁S

Guidance literature:: Multi-step reaction with 6 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C / Cooling with ice

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

6: water; lithium hydroxide / tetrahydrofuran; methanol / 0 °C

With 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm301630s