Technology Process of C37H49N3O3
There total 10 articles about C37H49N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
at 80 ℃;
for 0.5h;
DOI:10.1021/jm900305z
- Guidance literature:
-
With
hydrazine;
In
ethanol;
at 70 ℃;
for 0.5h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum tri-tert-butoxide; butanone / toluene / 16 h / 75 °C
1.2: 3.5 h / 20 - 49 °C
2.1: hydrogen / palladium 10% on activated carbon / pyridine / 20 °C / 760.05 Torr
3.1: triethylamine / tetrahydrofuran / 1 h / 20 °C
4.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 20 °C
4.2: 48 h / 20 °C
5.1: hydrazine / ethanol / 0.5 h / 70 °C
With
potassium tert-butylate; hydrogen; aluminum tri-tert-butoxide; triethylamine; butanone; hydrazine;
palladium 10% on activated carbon;
In
tetrahydrofuran; pyridine; ethanol; toluene; tert-butyl alcohol;