Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)]

Base Information

Chemical Name:Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)]
CAS No.:194282-81-0
Molecular Formula:C₇H₂Cl₃N₂*C₁₂H₆N₂O₄*C₂₁H₁₇N₅*Na*Ru
Molecular Weight:926.115
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)]

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Technology Process of Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)]

There total 1 articles about Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: thallium 2,4,5-trichlorophenylcyanamidate

: 194282-79-6
Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)I]

: 194282-81-0
Na[Ru(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)(2,2'-bipyridine-5,5'-dicarboxylate)(2,4,5-trichlorophenylcyanoamidate)]

Guidance literature:: In methanol; byproducts: TlI; Ar-atmosphere, exclusion of light; excess cyanamidate, refluxing for 4 h; cooling, centrifugation off of TlI, pptn. with Et2O, collection (filtration), washing (Et2O/MeOH=5:2, Et2O), drying; elem. anal.;
DOI:10.1016/s0020-1693(97)05457-1