6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine

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Chemical Name:6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine
CAS No.:1612222-54-4
Molecular Formula:C₂₄H₃₀N₆O₆
Molecular Weight:498.539
Hs Code.:

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Chemical Property of 6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine

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Technology Process of 6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine

There total 4 articles about 6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1612222-39-5
3-azido-1-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)propan-2-ol

: 1612222-54-4
6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 100 °C / Inert atmosphere

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo500890w

Reference yield:

: 23202-83-7,2592-42-9
5-benzyl-1,2-O-isopropylidene-α-D-xylofuranose

: 1612222-54-4
6-(4-(5-O-benzyl-3-O-methylene-1,2-O-isopropylidene-α-D-xylofuranose)-1H-1,2,3-triazol-1-yl)-6,7-dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]oxazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 20 °C / Inert atmosphere

2.1: sodium azide; Cu*O₄S^(2-)*5H₂O; sodium L-ascorbate / water / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

3.2: 12 h / 0 - 20 °C / Inert atmosphere

4.1: N,N-dimethyl-formamide / 100 °C / Inert atmosphere

With sodium azide; Cu*O₄S^(2-)*5H₂O; sodium hydride; sodium L-ascorbate; In water; N,N-dimethyl-formamide;
DOI:10.1021/jo500890w