[Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10]

Base Information

• Chemical Name: [Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10]
• CAS No.: 674316-56-4
• Molecular Formula: C₂₁H₁₀N₂O₁₀Os₃
• Molecular Weight: 1020.92

Synonyms:

Chemical Property of [Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10]

Chemical Property:

Purity/Quality:

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Technology Process of [Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10]

There total 1 articles about [Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

6-phenylpyridin-2-amine (39774-25-9) + bis(acetonitrile)decacarbonyltriosmium → dodecacarbonyl triosmium (15696-40-9) + [Os3(μ-H)(μ3-η2-HapyPh-N,N)(CO)9] + [Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10] (674316-56-4,674316-54-2) + [Os3(μ-H)(μ-η1-HapyPh-N)(CO)10]

Guidance literature:

In tetrahydrofuran; under N2 atm. soln. (Os3(CO)10(MeCN)2) and H2apyPh in THF was stirred atroom temp. for 4.5 h; solvent was removed in vacuo, residue was dissolved in CH2Cl2 and separated by TLC on silica (hexane-CH2Cl2 2:1); elem. anal.;

DOI:10.1021/om034040y

Reference yield: 90.0%

[Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10] (674316-56-4,674316-54-2) → [Os3(μ-H)(μ3-η2-HapyPh-N,N)(CO)9]

Guidance literature:

In tetrahydrofuran; Irradiation (UV/VIS); soln. (Os3(μ-H)(μ-η2-HapyPh-N,N)(CO)10) in THF was irradiated with UV light (400 W mercury lamp) for 5 min with gentle bubbling N2 through soln.; solvent was removed in vacuo, residue was washed with hexane; elem. anal.;

DOI:10.1021/om034040y

upstream raw materials:

6-phenylpyridin-2-amine

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