Technology Process of C30H36N2O3
There total 11 articles about C30H36N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;
for 2h;
DOI:10.1021/jm400542h
- Guidance literature:
-
Multi-step reaction with 9 steps
1: dichloromethane; tetrahydrofuran / 0.67 h / 20 °C
2: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C
3: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C
4: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C
5: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C
6: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C
7: 29 h / Reflux
8: potassium carbonate / methanol / 14 h / 20 °C
9: triethylamine / dichloromethane / 2 h / 0 °C
With
hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
1: |Grignard Reaction / 4: |Dess-Martin Oxidation;
DOI:10.1021/jm400542h
- Guidance literature:
-
Multi-step reaction with 8 steps
1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C
2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C
4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C
5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C
6: 29 h / Reflux
7: potassium carbonate / methanol / 14 h / 20 °C
8: triethylamine / dichloromethane / 2 h / 0 °C
With
hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
3: |Dess-Martin Oxidation;
DOI:10.1021/jm400542h