C₁₂H₁₀BrNO₂S

Base Information

Chemical Name:C₁₂H₁₀BrNO₂S
CAS No.:1423703-61-0
Molecular Formula:C₁₂H₁₀BrNO₂S
Molecular Weight:312.187
Hs Code.:

C<sub>12</sub>H<sub>10</sub>BrNO<sub>2</sub>S

Synonyms:

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Chemical Property of C₁₂H₁₀BrNO₂S

Chemical Property:

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Technology Process of C₁₂H₁₀BrNO₂S

There total 1 articles about C₁₂H₁₀BrNO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87943-97-3
ethyl 2-bromo-3-(4-bromophenyl)-3-oxopropanoate

: 1423703-61-0
C₁₂H₁₀BrNO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 2 h / 75 °C

2: hypophosphorous acid; sodium nitrite / water / 0 - 25 °C

With hypophosphorous acid; sodium nitrite; In ethanol; water;

Reference yield:

: 1423703-61-0
C₁₂H₁₀BrNO₂S

: 1423692-01-6
C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium hydroxide / methanol / 3 h / 20 °C

1.2: pH Ca_. 3

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

4.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

4.2: 0 °C / pH 4

5.1: sodium hydroxide / water; acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; diphenyl phosphoryl azide; water; sodium carbonate; triethylamine; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; toluene; acetonitrile;

Reference yield:

: 1423703-61-0
C₁₂H₁₀BrNO₂S

: 1423703-65-4
C₁₈H₁₅BrN₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / methanol / 3 h / 20 °C

1.2: pH Ca_. 3

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

With diphenyl phosphoryl azide; water; triethylamine; sodium hydroxide; In methanol; toluene;