Technology Process of C35H39N2O2(1+)*C7H7O3S(1-)
There total 4 articles about C35H39N2O2(1+)*C7H7O3S(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride / dichloromethane / 2 h / Reflux; Inert atmosphere
2: triethylamine; dmap / dichloromethane / 72 h / 20 °C
3: acetonitrile / 72 h / Reflux
With
dmap; oxalyl dichloride; triethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201201625
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium diacetate; potassium carbonate; N,N-dimethyl-L-alanine / N,N-dimethyl-formamide / 6 h / Reflux
2: oxalyl dichloride / dichloromethane / 2 h / Reflux; Inert atmosphere
3: triethylamine; dmap / dichloromethane / 72 h / 20 °C
4: acetonitrile / 72 h / Reflux
With
dmap; oxalyl dichloride; N,N-dimethyl-L-alanine; palladium diacetate; potassium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201201625
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; dmap / dichloromethane / 72 h / 20 °C
2: acetonitrile / 72 h / Reflux
With
dmap; triethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201201625