WCl₃(PhC₂Ph)(PMe₃)2

Base Information

Chemical Name:WCl₃(PhC₂Ph)(PMe₃)2
CAS No.:143281-01-0
Molecular Formula:C₂₀H₂₈Cl₃P₂W
Molecular Weight:620.599
Hs Code.:

WCl<sub>3</sub>(PhC<sub>2</sub>Ph)(PMe<sub>3</sub>)2

Synonyms:

Suppliers and Price of WCl₃(PhC₂Ph)(PMe₃)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of WCl₃(PhC₂Ph)(PMe₃)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of WCl₃(PhC₂Ph)(PMe₃)2

There total 2 articles about WCl₃(PhC₂Ph)(PMe₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2W⁽⁴⁺⁾*8Cl^(1-)*2C₆H₅CCC₆H₅={WCl₄((C₆H₅)CC(C₆H₅))}2

: 594-09-2
trimethylphosphane

: 143281-01-0
WCl₃(C₆H₅CCC₆H₅)(P(CH₃)3)2

Guidance literature:: With sodium amalgam; In benzene; stirring of W-complex with 1 equiv. of Na-amalgam and excess PMe3 (2 h); filtration, washing (C6H6), evapn., dissoln. in MePh, crystn. on slow evapn.; elem. anal.;
DOI:10.1039/DT9950001153

Reference yield:

: 2W⁽⁴⁺⁾*8Cl^(1-)*2C₆H₅CCC₆H₅={WCl₄((C₆H₅)CC(C₆H₅))}2

: 594-09-2
trimethylphosphane

: 143281-01-0
WCl₃(PhC₂Ph)(PMe₃)2

Guidance literature:: With sodium amalgam; In benzene;
DOI:10.1016/S0277-5387(00)83375-6

Reference yield: 83.0%

: 143281-01-0
WCl₃(PhC₂Ph)(PMe₃)2

: 764-35-2
2-Hexyne

: WCl₂(C₆H₅CCC₆H₅)(CH₃CCC₃H₇)(P(CH₃)3)2*0.167C₆H₆

Guidance literature:: With Na#Hg; benzene; In benzene; sodium amalgame was added to a soln. of the complex and hex-2-yne in benzene, stirred for 1.5 h; filtered, extd. with benzene, extracts and filtrate were combined, volatiles were removed, stored under light petroleum; elem. anal.;
DOI:10.1039/DT9940001783