C₃₁H₂₄F₆I₂S₂

Base Information

• Chemical Name: C₃₁H₂₄F₆I₂S₂
• CAS No.: 1338799-61-3
• Molecular Formula: C₃₁H₂₄F₆I₂S₂
• Molecular Weight: 828.463
• Mol file: 1338799-61-3.mol

Synonyms:

Chemical Property of C₃₁H₂₄F₆I₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₂₄F₆I₂S₂

There total 7 articles about C₃₁H₂₄F₆I₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dibromo-2-methylthiophene (29421-73-6) → C31H24F6I2S2 (1338799-61-3)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride; n-butyllithium; Triisopropyl borate / tetrahydrofuran; water / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water

3: n-butyllithium / tetrahydrofuran / -78 °C

4: Iodine monochloride / dichloromethane

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Triisopropyl borate; Iodine monochloride; sodium carbonate; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/ja207025x

Reference yield:

C16H21BrSSi (1338799-59-9) → C31H24F6I2S2 (1338799-61-3)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: Iodine monochloride / dichloromethane

With n-butyllithium; Iodine monochloride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja207025x

Reference yield:

2-Methylthiophene (554-14-3) → C31H24F6I2S2 (1338799-61-3)

Guidance literature:

Multi-step reaction with 5 steps

1: bromine; acetic acid

2: hydrogenchloride; n-butyllithium; Triisopropyl borate / tetrahydrofuran; water / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water

4: n-butyllithium / tetrahydrofuran / -78 °C

5: Iodine monochloride / dichloromethane

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Triisopropyl borate; bromine; Iodine monochloride; sodium carbonate; acetic acid; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/ja207025x

upstream raw materials:

2-Methylthiophene

3,5-dibromo-2-methylthiophene

C₁₆H₂₁BrSSi

C₃₇H₄₂F₆S₂Si₂

Downstream raw materials:

C₄₅H₃₈F₆INO₂S₂

C₅₉H₅₂F₆N₂O₄S₂