C₆₆H₇₀N₈O₄

Base Information

• Chemical Name: C₆₆H₇₀N₈O₄
• CAS No.: 1538555-42-8
• Molecular Formula: C₆₆H₇₀N₈O₄
• Molecular Weight: 1039.33
• Mol file: 1538555-42-8.mol

Synonyms:

Chemical Property of C₆₆H₇₀N₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₆H₇₀N₈O₄

There total 11 articles about C₆₆H₇₀N₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-Dibromoanthracene (523-27-3) → C66H70N8O4 (1538555-42-8)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium carbonate; water; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 24 h / Inert atmosphere; Reflux

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux

3.1: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 66 °C

5.1: dichloromethane / 5 h / 20 °C

5.2: 20 °C

5.3: 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

6.3: 20 °C / Inert atmosphere

With N-Bromosuccinimide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; water; sodium carbonate; potassium carbonate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: |Suzuki Coupling;

DOI:10.1039/c3cc48618d

Reference yield:

1,2-bis-[4-(bromomethyl)phenyl]-1,2-diphenylethene (1053241-67-0) → C66H70N8O4 (1538555-42-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 66 °C

3.1: dichloromethane / 5 h / 20 °C

3.2: 20 °C

3.3: 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c3cc48618d

Reference yield:

1,2-bis-(4-(azidomethyl)phenyl)-1,2-diphenylethene (1054451-33-0) → C66H70N8O4 (1538555-42-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 66 °C

2.1: dichloromethane / 5 h / 20 °C

2.2: 20 °C

2.3: 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

3.3: 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c3cc48618d

upstream raw materials:

C₂₈H₂₀N₆

C₂₈H₂₄N₂

9,10-Dibromoanthracene

4-Methylbenzophenone