C₆₉H₆₇F₂N₆O₁₀P

Base Information

Chemical Name:C₆₉H₆₇F₂N₆O₁₀P
CAS No.:1613591-48-2
Molecular Formula:C₆₉H₆₇F₂N₆O₁₀P
Molecular Weight:1209.3
Hs Code.:

C<sub>69</sub>H<sub>67</sub>F<sub>2</sub>N<sub>6</sub>O<sub>10</sub>P

Synonyms:

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Chemical Property of C₆₉H₆₇F₂N₆O₁₀P

Chemical Property:

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Technology Process of C₆₉H₆₇F₂N₆O₁₀P

There total 20 articles about C₆₉H₆₇F₂N₆O₁₀P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613589-70-0
9-(2,5-dideoxy-2-fluoro-2-C-methyl-5-iodo-β-D-ribofuranosyl)-6-ethoxy-2-((4-monomethoxytrityl)amino)purine

: 1613591-48-2
C₆₉H₆₇F₂N₆O₁₀P

Guidance literature:: Multi-step reaction with 6 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

2: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

3: silver nitrate / dichloromethane / 0 - 20 °C

4: 15-crown-5 / N,N-dimethyl-formamide / 72 h / 95 °C

5: ammonia / methanol / 18 h / 20 °C

6: 1-methyl-1H-imidazole / dichloromethane; acetonitrile / 10 h / 20 °C

With 1-methyl-1H-imidazole; N-iodo-succinimide; 15-crown-5; ammonia; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1613589-72-2
9-(2,5-dideoxy-2,4-difluoro-5-iodo-2-C-methyl-β-D-ribofuranosyl)-6-ethoxy-2-((4-monomethoxytrityl)amino)purine

: 1613591-48-2
C₆₉H₆₇F₂N₆O₁₀P

Guidance literature:: Multi-step reaction with 4 steps

1: silver nitrate / dichloromethane / 0 - 20 °C

2: 15-crown-5 / N,N-dimethyl-formamide / 72 h / 95 °C

3: ammonia / methanol / 18 h / 20 °C

4: 1-methyl-1H-imidazole / dichloromethane; acetonitrile / 10 h / 20 °C

With 1-methyl-1H-imidazole; 15-crown-5; ammonia; silver nitrate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1613589-69-7
9-(2-deoxy-2-fluoro-2-C-methyl-β-D-ribofuranosyl)-6-ethoxy-2-((4-monomethoxytrityl)amino)purine

: 1613591-48-2
C₆₉H₆₇F₂N₆O₁₀P

Guidance literature:: Multi-step reaction with 7 steps

1: triphenylphosphine; pyridine; iodine / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

3: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

4: silver nitrate / dichloromethane / 0 - 20 °C

5: 15-crown-5 / N,N-dimethyl-formamide / 72 h / 95 °C

6: ammonia / methanol / 18 h / 20 °C

7: 1-methyl-1H-imidazole / dichloromethane; acetonitrile / 10 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; N-iodo-succinimide; 15-crown-5; ammonia; iodine; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;