1-trityl-4-phenylazoimidazole

Base Information

• Chemical Name: 1-trityl-4-phenylazoimidazole
• CAS No.: 1367346-22-2
• Molecular Formula: C₂₈H₂₂N₄
• Molecular Weight: 414.509
• Mol file: 1367346-22-2.mol

Synonyms:

Chemical Property of 1-trityl-4-phenylazoimidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-trityl-4-phenylazoimidazole

There total 4 articles about 1-trityl-4-phenylazoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-5-(phenyldiazenyl)-1H-imidazole (1367346-16-4) → 1-trityl-4-phenylazoimidazole (1367346-22-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / acetontrile / 3 h / Reflux

2: UV-irradiation

With triethylamine; In acetontrile;

DOI:10.1021/jo202688x

Reference yield:

C19H31N5O2SSi → 1-trityl-4-phenylazoimidazole (1367346-22-2)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride; cesium fluoride / tetrahydrofuran / 2 h / 20 °C

2: hydrogenchloride; water / ethanol / 3 h / 80 °C

3: triethylamine / acetontrile / 3 h / Reflux

4: UV-irradiation

With hydrogenchloride; tetrabutyl ammonium fluoride; water; triethylamine; cesium fluoride; In tetrahydrofuran; acetontrile; ethanol;

DOI:10.1021/jo202688x

Reference yield:

1-dimethylsulfamoyl-5-phenylazoimidazole (1367346-15-3) → 1-trityl-4-phenylazoimidazole (1367346-22-2)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; water / ethanol / 3 h / 80 °C

2: triethylamine / acetontrile / 3 h / Reflux

3: UV-irradiation

With hydrogenchloride; water; triethylamine; In acetontrile; ethanol;

DOI:10.1021/jo202688x

upstream raw materials:

1-dimethylsulfamoyl-5-phenylazoimidazole

(E)-5-(phenyldiazenyl)-1H-imidazole

1-trityl-4-phenylazoimidazole