Technology Process of C16H24O4
There total 6 articles about C16H24O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
at 80 ℃;
for 2h;
DOI:10.1021/jo0159035
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 74 percent / KF / methanol / 16 h / 25 °C
2.1: 74 percent / p-TsOH / benzene / 4 h / Heating
3.1: 82 percent / CeCl3; NaBH4 / ethanol / 2 h / 0 - 25 °C
4.1: NaH / tetrahydrofuran / 3 h / 25 °C
4.2: 697 mg / tetrahydrofuran / 0.5 h / 25 °C
5.1: 344 mg / Bu3SnH; AIBN / benzene / 2 h / 80 °C
With
potassium fluoride; sodium tetrahydroborate; cerium(III) chloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; ethanol; benzene;
DOI:10.1021/jo0159035
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 56 percent / Jones reagent / acetone / 6 h / 0 - 25 °C
2.1: 74 percent / KF / methanol / 16 h / 25 °C
3.1: 74 percent / p-TsOH / benzene / 4 h / Heating
4.1: 82 percent / CeCl3; NaBH4 / ethanol / 2 h / 0 - 25 °C
5.1: NaH / tetrahydrofuran / 3 h / 25 °C
5.2: 697 mg / tetrahydrofuran / 0.5 h / 25 °C
6.1: 344 mg / Bu3SnH; AIBN / benzene / 2 h / 80 °C
With
potassium fluoride; sodium tetrahydroborate; jones reagent; cerium(III) chloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; ethanol; acetone; benzene;
1.1: Jones oxidation;
DOI:10.1021/jo0159035
