C₂₉H₄₇N₂O₇PS

Base Information

Chemical Name:C₂₉H₄₇N₂O₇PS
CAS No.:1402829-90-6
Molecular Formula:C₂₉H₄₇N₂O₇PS
Molecular Weight:598.741
Hs Code.:

C<sub>29</sub>H<sub>47</sub>N<sub>2</sub>O<sub>7</sub>PS

Synonyms:

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Chemical Property of C₂₉H₄₇N₂O₇PS

Chemical Property:

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Technology Process of C₂₉H₄₇N₂O₇PS

There total 8 articles about C₂₉H₄₇N₂O₇PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1809-19-4
dibutyl hydrogen phosphite

: 159005-71-7
N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-N-isobutyl-4-methoxybenzenesulfonamide

: 1402829-90-6
C₂₉H₄₇N₂O₇PS

Guidance literature:: With potassium carbonate; In tetrachloromethane; dichloromethane;
DOI:10.1002/cmdc.201200271

Reference yield:

: 169331-42-4
βS--αR-<<(2-methylpropyl)amino>methyl>-benzenepropanol

: 1402829-90-6
C₂₉H₄₇N₂O₇PS

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / water; dichloromethane / 3 h / 0 - 20 °C

2: Pd(OH)2/C; hydrogen / methanol / 24 h / 20 °C / 760.05 Torr

3: potassium carbonate / dichloromethane; tetrachloromethane

With Pd(OH)2/C; hydrogen; sodium carbonate; potassium carbonate; In methanol; tetrachloromethane; dichloromethane; water; 3: |Atherton-Todd Synthesis;
DOI:10.1002/cmdc.201200271

Reference yield:

: 111060-52-7
(S)-2-(dibenzylamino)-3-phenylpropan-1-ol

: 1402829-90-6
C₂₉H₄₇N₂O₇PS

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 - 0 °C

1.2: 1 h

2.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / -20 °C

3.1: 1H-imidazole / dichloromethane / 0 - 20 °C

4.1: diisobutylaluminium hydride / diethyl ether; hexane / 3 h / -78 °C

4.2: 3 h / 20 °C

4.3: 20 °C / Cooling with ice

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

6.1: sodium carbonate / water; dichloromethane / 3 h / 0 - 20 °C

7.1: Pd(OH)2/C; hydrogen / methanol / 24 h / 20 °C / 760.05 Torr

8.1: potassium carbonate / dichloromethane; tetrachloromethane

With 1H-imidazole; oxalyl dichloride; Pd(OH)2/C; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; hexane; dichloromethane; water; 1.1: |Swern Oxidation / 8.1: |Atherton-Todd Synthesis;
DOI:10.1002/cmdc.201200271