(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-glucopyranoside

Base Information

Chemical Name:(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-glucopyranoside
CAS No.:131904-51-3
Molecular Formula:C₄₈H₅₉NO₁₈
Molecular Weight:938.984
Hs Code.:

(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl-<methyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosyl)onate>-(2-6)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-glucopyranoside

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Technology Process of (6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-glucopyranoside

There total 20 articles about (6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 67670-69-3
N-acetyl-4,7,8,9-tetra-O-acetyl-2-chloro-2-deoxyneuraminic acid methyl ester

: 131904-50-2
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

: 131904-51-3,132015-21-5,132015-24-8,132072-02-7
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-galactopyranoside

: 131904-51-3,132015-21-5,132015-24-8,132072-02-7
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In dichloromethane; for 22h; Ambient temperature;
DOI:10.1021/jo00005a015

Reference yield: 13.0%

: 67670-69-3
N-acetyl-4,7,8,9-tetra-O-acetyl-2-chloro-2-deoxyneuraminic acid methyl ester

: 131904-50-2
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

: 131904-51-3,132015-21-5,132015-24-8,132072-02-7
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-galactopyranoside

: 131904-51-3,132015-21-5,132015-24-8,132072-02-7
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In dichloromethane; for 22h; Ambient temperature;
DOI:10.1021/jo00005a015

Reference yield:

: 35669-28-4
(6S)-<6-2H>Methyl-β-D-galactopyranoside

: 131904-51-3,132015-21-5,132015-24-8,132072-02-7
(6S)-<6-2H>Methyl 2,3,4-tri-O-benzyl--(2-6)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NEt₃, 4-(dimethylamino)pyridine / dimethylformamide / 3 h / Ambient temperature

2: NaH, NEt₃ / dimethylformamide / 6 h / Ambient temperature

3: tetrabutylammonium fluoride / tetrahydrofuran; ethanol / 3 h / Heating

4: 13 percent / HgBr₂, Hg(CN)2, mol. sieve 4A / CH₂Cl₂ / 22 h / Ambient temperature

With dmap; 4 A molecular sieve; tetrabutyl ammonium fluoride; mercury(II) cyanide; sodium hydride; triethylamine; mercury dibromide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00005a015