cis-1-Chlor-1,3-diphenylpropen

Base Information

• Chemical Name: cis-1-Chlor-1,3-diphenylpropen
• CAS No.: 51117-49-8
• Molecular Formula: C₁₅H₁₃Cl
• Molecular Weight: 228.721
• Mol file: 51117-49-8.mol

Synonyms:

Chemical Property of cis-1-Chlor-1,3-diphenylpropen

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-1-Chlor-1,3-diphenylpropen

There total 3 articles about cis-1-Chlor-1,3-diphenylpropen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloride (100-44-7) + phenylacetylene (536-74-3) → cis-1-Chlor-1,3-diphenylpropen (51117-49-8) + trans-1-Chlor-1,3-diphenylpropen (51117-50-1)

Guidance literature:

With iron(III) chloride hexahydrate; In dichloromethane; at 50 ℃; for 12h; optical yield given as %de;

DOI:10.1002/adsc.200800708

Reference yield:

1-chloro-3-phenyl-2-propyne (3355-31-5) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 1,3-diphenyl-1-propyne (4980-70-5) + cis-1-Chlor-1,3-diphenylpropen (51117-49-8) + trans-1-Chlor-1,3-diphenylpropen (51117-50-1)

Guidance literature:

With aluminium trichloride; In benzene; at 10 ℃;

Reference yield:

→ cis-1-Chlor-1,3-diphenylpropen (51117-49-8)

Guidance literature:

Butyrophenon, PCl5 in sd. CCl4 (30 Min.) (neben anderen Prodd.; Nicht rein erhalten);

upstream raw materials:

1-chloro-3-phenyl-2-propyne

benzene

benzyl chloride

phenylacetylene