endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid

Base Information

Chemical Name:endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid
CAS No.:55449-71-3
Molecular Formula:C₈H₁₂O
Molecular Weight:124.183
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid

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Technology Process of endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid

There total 8 articles about endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 930-99-4
(3aS,6aS)-1,2,3,3a,4,6a-Hexahydro-pentalene

: 6567-98-2,24454-41-9,24454-42-0,55449-70-2,55449-71-3
(1bR,4aR)-Octahydro-1-oxa-cyclopropa[a]pentalene

Guidance literature:: With 1-methyl-pyrrolidin-2-one; 18-crown-6 ether; dihydrogen peroxide; sodium carbonate; trichlorophosphate; In dichloromethane; 1) -20 deg C, 1h, 2) -20 deg C, to 20 deg C;
DOI:10.1021/jo00001a095

Reference yield: 53.0%

: 5549-09-7
bicyclo[3.3.0]oct-2-ene

: 6567-98-2,24454-41-9,24454-42-0,55449-70-2,55449-71-3
(+/-)-2β,3β-epoxy-1α,2β,3β,5α-bicyclo[3.3.0]oct-2-eneoxirane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; Heating;
DOI:10.1021/jo9615155

Reference yield:

: 930-99-4
(3aS,6aS)-1,2,3,3a,4,6a-Hexahydro-pentalene

: 6567-98-2,24454-41-9,24454-42-0,55449-70-2,55449-71-3
(+/-)-2β,3β-epoxy-1α,2β,3β,5α-bicyclo[3.3.0]oct-2-eneoxirane

: 6567-98-2,24454-41-9,24454-42-0,55449-70-2,55449-71-3
endo-2,3-Epoxy-cis-bicyclo<3.3.0>octan; endo-cis-Bicyclo<3.3.0>octen-(2)-oxid

Guidance literature:: With sodium hydroxide; N-Bromosuccinimide; Yield given. Multistep reaction. Yields of byproduct given; 1) DMSO-H₂O, room temp., 2) H₂O, room temp.;
DOI:10.1016/0040-4039(84)80040-4