C₄₈H₅₃N₃O₇

Base Information

Chemical Name:C₄₈H₅₃N₃O₇
CAS No.:1322684-97-8
Molecular Formula:C₄₈H₅₃N₃O₇
Molecular Weight:783.965
Hs Code.:

C<sub>48</sub>H<sub>53</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₅₃N₃O₇

Chemical Property:

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Technology Process of C₄₈H₅₃N₃O₇

There total 7 articles about C₄₈H₅₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1322684-96-7
C₅₀H₅₅N₃O₈

: 1322684-97-8
C₄₈H₅₃N₃O₇

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 20 ℃; for 1.5h;
DOI:10.1246/bcsj.20100340

Reference yield:

: 1322684-95-6
6-{4-[3-(4-methoxyphenyl)-4-nitrobutanoyl]phenoxy}hexyl acetate

: 1322684-97-8
C₄₈H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 24 h / Reflux

2: lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / 20 °C

With lithium hydroxide monohydrate; ammonium acetate; In tetrahydrofuran; ethanol; water;
DOI:10.1246/bcsj.20100340

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 1322684-97-8
C₄₈H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / 90 °C / Inert atmosphere

2: sodium hydroxide / methanol / 5 h / Inert atmosphere; Reflux

3: potassium hydroxide / methanol / 24 h / Reflux

4: dmap; triethylamine / dichloromethane / 18 h / 0 - 20 °C

5: ammonium acetate / ethanol / 24 h / Reflux

6: lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / 20 °C

With dmap; lithium hydroxide monohydrate; ammonium acetate; potassium carbonate; triethylamine; potassium iodide; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 3: Michael addition;
DOI:10.1246/bcsj.20100340