diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I)

Base Information

Chemical Name:diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I)
CAS No.:1002356-23-1
Molecular Formula:C₅₁H₃₉N₂O₂P₂Re
Molecular Weight:960.037
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I)

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Technology Process of diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I)

There total 1 articles about diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 13228-40-5
2-(2-pyridinyl)-1H-indole

: 14220-21-4
rhenium(I) pentacarbonyl bromide

: 603-35-0
triphenylphosphine

: 1002356-23-1
diacarbonyl[2-(2'-pyridyl)indolido-N,N']bis(triphenylphosphane)rhenium(I)

Guidance literature:: With Et₃N; In toluene; byproducts: Et3NHCl, CO; under Ar, Schlen k techniques; soln. of metal compd. (0.2 mmol), ligand (0.2 mmol), PPh3 (0.4 mmol) and Et3N (0.22 mmol) in toluene, stirred at100°C for 48 h; crystd. (-32°C, overnight), septd., chromd. (SiO2, CH2Cl2), elem.anal.;
DOI:10.1002/ejic.200600730