Phenylimino-3,3'-bis

Base Information

• Chemical Name: Phenylimino-3,3'-bis
• CAS No.: 73627-58-4
• Molecular Formula: C₁₄H₂₅NO₄P₂
• Molecular Weight: 333.304

Synonyms:

Chemical Property of Phenylimino-3,3'-bis

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Phenylimino-3,3'-bis

There total 4 articles about Phenylimino-3,3'-bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

aniline (62-53-3) + 2-Methyl-2-oxo-1,2-oxaphospholan (53314-66-2) → Phenylimino-3,3'-bis (73627-58-4)

Guidance literature:

at 200 ℃; for 9h;

Reference yield: 66.0%

(3-Anilinopropyl)methylphosphinsaeure (73627-59-5) + 2-Methyl-2-oxo-1,2-oxaphospholan (53314-66-2) → Phenylimino-3,3'-bis (73627-58-4)

Guidance literature:

at 200 ℃; for 6h;

Reference yield:

(3-Anilinopropyl)methylphosphinsaeure (73627-59-5) → Phenylimino-3,3'-bis (73627-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 g / 250 °C / 0.5 Torr

2: 70 percent / 9 h / 200 °C

upstream raw materials:

aniline

2-Methyl-2-oxo-1,2-oxaphospholan

(3-Anilinopropyl)methylphosphinsaeure

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