C₁₅H₂₀O₇

Base Information

Chemical Name:C₁₅H₂₀O₇
CAS No.:99268-19-6
Molecular Formula:C₁₅H₂₀O₇
Molecular Weight:312.32
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀O₇

Chemical Property:

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Technology Process of C₁₅H₂₀O₇

There total 12 articles about C₁₅H₂₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 99268-18-5
C₁₅H₂₀O₆

: 99268-19-6
C₁₅H₂₀O₇

Guidance literature:: With sodium chlorite; aminosulfonic acid; In 1,4-dioxane; water; at 25 ℃; for 0.5h;
DOI:10.1021/ja00310a076

Reference yield:

: 51557-85-8
2-allyl-2-cyclopenten-1-one

: 99268-19-6
C₁₅H₂₀O₇

Guidance literature:: Multi-step reaction with 12 steps

1: 1.) Me₂LiCu*SMe₂; 2.) 10percent KOH / 1.) Et₂O, -30 deg C; 2.) EtOH, reflux, 40 min

2: dimethylformamide / 2 h / 130 °C

3: 0.17 h / 0 °C

4: 60 percent / 2.) MeOH / 2.) conc. HCl / 1.) Et₂O, -78 deg C, 1 h; 2.) 25 deg C, 2 h

5: 1.) LDA, HMPA / tetrahydrofuran / 1.) -78 deg C; 2.) 25 deg C

6: LiAlH₄ / diethyl ether / 0.25 h / 25 °C

7: 1.) KIO₄, K₂CO₃, KMnO₄; 2.) p-TsOH / 1.) aq. t-BuOH, 25 deg C, 60 h; 2.) C₆H₆, reflux, 20 min

8: 75 percent / CH₃SO₃H / CH₂Cl₂ / 46 h / Heating

9: 1.) BBr₃; 2.) PDC / 1.) CH₂Cl₂, -78 deg C, 3 min; 2.) CH₂Cl₂, 25 deg C, 24 h

10: 37 percent / OsO₄ / pyridine / 0.5 h / 25 °C

11: CF₃CO₃H / CH₂Cl₂ / 0.25 h / 0 °C

12: 76 percent / NaClO₂, NH₂SO₂OH / dioxane; H₂O / 0.5 h / 25 °C

With methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium chlorite; potassium permanganate; osmium(VIII) oxide; lithium aluminium tetrahydride; dipyridinium dichromate; potassium metaperiodate; methanesulfonic acid; trifluoroacetyl peroxide; aminosulfonic acid; boron tribromide; potassium carbonate; Lithium dimethylcuprate-dimethyl sulfide complex; toluene-4-sulfonic acid; lithium diisopropyl amide; hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; pyridine; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00310a076

Reference yield:

: 99268-09-4
(1S,7aS)-7a-Allyl-1-methyl-1,2,3,6,7,7a-hexahydro-inden-5-one

: 99268-19-6
C₁₅H₂₀O₇

Guidance literature:: Multi-step reaction with 11 steps

1: dimethylformamide / 2 h / 130 °C

2: 0.17 h / 0 °C

3: 60 percent / 2.) MeOH / 2.) conc. HCl / 1.) Et₂O, -78 deg C, 1 h; 2.) 25 deg C, 2 h

4: 1.) LDA, HMPA / tetrahydrofuran / 1.) -78 deg C; 2.) 25 deg C

5: LiAlH₄ / diethyl ether / 0.25 h / 25 °C

6: 1.) KIO₄, K₂CO₃, KMnO₄; 2.) p-TsOH / 1.) aq. t-BuOH, 25 deg C, 60 h; 2.) C₆H₆, reflux, 20 min

7: 75 percent / CH₃SO₃H / CH₂Cl₂ / 46 h / Heating

8: 1.) BBr₃; 2.) PDC / 1.) CH₂Cl₂, -78 deg C, 3 min; 2.) CH₂Cl₂, 25 deg C, 24 h

9: 37 percent / OsO₄ / pyridine / 0.5 h / 25 °C

10: CF₃CO₃H / CH₂Cl₂ / 0.25 h / 0 °C

11: 76 percent / NaClO₂, NH₂SO₂OH / dioxane; H₂O / 0.5 h / 25 °C

With methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium chlorite; potassium permanganate; osmium(VIII) oxide; lithium aluminium tetrahydride; dipyridinium dichromate; potassium metaperiodate; methanesulfonic acid; trifluoroacetyl peroxide; aminosulfonic acid; boron tribromide; potassium carbonate; toluene-4-sulfonic acid; lithium diisopropyl amide; hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; pyridine; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00310a076