Technology Process of C54H53N13O10S6
There total 8 articles about C54H53N13O10S6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2.1: chloroformic acid ethyl ester; triethylamine / acetone / 1 h
2.2: 1.33 h / 60 °C
3.1: 2 h / 80 °C
4.1: pyridine; dmap / 3 h
5.1: dichloromethane / 0.5 h
6.1: water; sodium hydrogencarbonate / ethyl acetate
7.1: pyridine
8.1: water; lithium hydroxide / tetrahydrofuran; methanol
With
pyridine; dmap; water; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; sodium hydroxide; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jm200938f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dichloromethane / 0.5 h
2: water; sodium hydrogencarbonate / ethyl acetate
3: pyridine
4: water; lithium hydroxide / tetrahydrofuran; methanol
With
pyridine; water; sodium hydrogencarbonate; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200938f
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2 h / 80 °C
2: pyridine; dmap / 3 h
3: dichloromethane / 0.5 h
4: water; sodium hydrogencarbonate / ethyl acetate
5: pyridine
6: water; lithium hydroxide / tetrahydrofuran; methanol
With
pyridine; dmap; water; sodium hydrogencarbonate; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200938f
