[(iPrO)2P(S)NC(S)NH]2-p-C₆H₄Co

Base Information

• Chemical Name: [(iPrO)2P(S)NC(S)NH]2-p-C₆H₄Co
• CAS No.: 784156-20-3
• Molecular Formula: C₂₀H₃₄N₄O₄P₂S₄*Co
• Molecular Weight: 643.719
• Mol file: 784156-20-3.mol

Synonyms:

Chemical Property of [(iPrO)2P(S)NC(S)NH]2-p-C₆H₄Co

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of [(iPrO)2P(S)NC(S)NH]2-p-C₆H₄Co

There total 1 articles about [(iPrO)2P(S)NC(S)NH]2-p-C₆H₄Co which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

cobalt(II) nitrate hexahydrate + [(iPrO)2P(S)NHC(S)NH]2-p-C6H4 (784156-09-8) → [(iPrO)2P(S)NC(S)NH]2-p-C6H4Co (784156-20-3)

Guidance literature:

With KOH; In ethanol; water; thiourea ligand in anhydrous EtOH mixed with ethanol soln. of KOH; Co(NO3)2*6H2O in water added dropwise with vigorous stirring; extracted with CH2Cl2; organic phase washed with water; solvent removed in vacuum; dried over MgSO4 as an acetone soln.; solvent removed in vacuum at 50°C, recrystn. from acetone/n-hexane; elem. anal.;

DOI:10.1016/j.poly.2004.07.005

upstream raw materials:

[(iPrO)2P(S)NHC(S)NH]2-p-C₆H₄