11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester
CAS No.:80143-19-7
Molecular Formula:C₅₃H₇₃N₅O₁₄
Molecular Weight:1004.19
Hs Code.:

11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of 11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of 11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

There total 2 articles about 11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 73341-44-3
N-carbobenzoxy-11-aminoundecanoic acid p-nitrophenyl ester

: 57816-11-2,62928-83-0,75283-21-5,76498-06-1,76498-09-4
benzyl 2-acetamido-2-deoxy-3-O-(D-2-propanoyl-L-alanyl-D-isoglutamine benzyl ester)-α-D-glucopyranoside

: 80143-19-7
11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With N-ethylmorpholine;; benzotriazol-1-ol; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1248/cpb.29.2215

Reference yield:

: 71811-18-2
N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-muramyl-α-aminoisobutyryl-D-isoglutamine benzyl ester

: 80143-19-7
11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / acetic acid (75percent) / 0.5 h / Heating

2: 50 percent / 1-hydroxybenzotriazole, N-ethylmorpholine / dimethylformamide / 16 h / Ambient temperature

With N-ethylmorpholine;; benzotriazol-1-ol; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.29.2215

Reference yield:

: 80143-19-7
11-Benzyloxycarbonylamino-undecanoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-{1-[1-((R)-3-benzyloxycarbonyl-1-carbamoyl-propylcarbamoyl)-1-methyl-ethylcarbamoyl]-ethoxy}-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

: C₄₃H₆₇N₅O₁₇

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / hydrogen / palladium black / acetic acid / 3 h / Ambient temperature

2: 59.4 percent / ethylmorpholine / dimethylformamide / 16 h / Ambient temperature

With 2-ethylmorpholine; hydrogen; palladium; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.29.2215