C₁₁H₁₅⁽²⁾H₂N

Base Information

• Chemical Name: C₁₁H₁₅⁽²⁾H₂N
• CAS No.: 1352167-46-4
• Molecular Formula: C₁₁H₁₇N
• Molecular Weight: 165.247
• Mol file: 1352167-46-4.mol

Synonyms:

Chemical Property of C₁₁H₁₅⁽²⁾H₂N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₅⁽²⁾H₂N

There total 2 articles about C₁₁H₁₅⁽²⁾H₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylbutyramide (10264-14-9) → C11H15(2)H2N (1352167-46-4)

Guidance literature:

With lithium aluminium deuteride; In tetrahydrofuran; at 0 ℃; Reflux;

DOI:10.1021/ja208860x

Reference yield:

benzylamine (100-46-9) → C11H15(2)H2N (1352167-46-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

2: lithium aluminium deuteride / tetrahydrofuran / 0 °C / Reflux

With lithium aluminium deuteride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja208860x

Reference yield:

C11H15(2)H2N (1352167-46-4) → C16H21(2)H2NO

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; sodium iodide / acetonitrile / 12 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Molecular sieve; Inert atmosphere

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; acetonitrile;

DOI:10.1021/ja208860x

upstream raw materials:

N-benzylbutyramide

benzylamine

Downstream raw materials:

C₁₆H₂₁⁽²⁾H₂NO

C₁₆H₂₁⁽²⁾H₂N