C₃₅H₂₇O₄P

Base Information

• Chemical Name: C₃₅H₂₇O₄P
• CAS No.: 1392425-99-8
• Molecular Formula: C₃₅H₂₇O₄P
• Molecular Weight: 542.571
• Mol file: 1392425-99-8.mol

Synonyms:

Chemical Property of C₃₅H₂₇O₄P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₇O₄P

There total 1 articles about C₃₅H₂₇O₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

dimethyl 9-bromofluorene-2,7-dicarboxylate (1216990-82-7) + triphenylphosphine (603-35-0) → C35H27O4P (1392425-99-8)

Guidance literature:

In toluene; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c2dt30195d

Reference yield:

C35H27O4P (1392425-99-8) → C32H30O8S (1392426-09-3)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene / 48 h / 60 °C / Inert atmosphere

2: toluene / -78 - 20 °C / Inert atmosphere

3: hexafluorophosphoric acid / dichloromethane / Inert atmosphere

With hexafluorophosphoric acid; In dichloromethane; toluene; 1: Wittig reaction;

DOI:10.1039/c2dt30195d

Reference yield:

C35H27O4P (1392425-99-8) → C32H29O8S(1-)*C34H43N2S(1+)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 48 h / 60 °C / Inert atmosphere

2: toluene / -78 - 20 °C / Inert atmosphere

In toluene; 1: Wittig reaction;

DOI:10.1039/c2dt30195d

upstream raw materials:

dimethyl 9-bromofluorene-2,7-dicarboxylate

triphenylphosphine

Downstream raw materials:

C₃₂H₃₀O₈S