Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

Base Information

Chemical Name:Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate
CAS No.:81502-06-9
Molecular Formula:C₃₀H₂₃N₂O₄S₂*Na
Molecular Weight:562.645
Hs Code.:

Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

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Chemical Property of Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

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Technology Process of Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

There total 3 articles about Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1008-72-6
sodium 2-formylbenzenesulfonate

: 81508-73-8
5-phenyl-9-benzylidene-2,3,6,7,8,9-hexahydro-5H-thiazolo-<2,3,-b>quinazolin-3-one

: 81502-06-9
Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

Guidance literature:: With sodium acetate; In acetic acid; Heating;

Reference yield:

: 81501-98-6
(8E)?8-benzylidene-3,4,5,6,7,8-hexahydro-4-phenylquinazoline-2(1H)-thione

: 81502-06-9
Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / potassium carbonate / ethanol / 6.5 h / Heating

2: 74 percent / conc. HCl / methanol / 12 h / Heating

3: 48 percent / sodium acetate / acetic acid / Heating

With hydrogenchloride; sodium acetate; potassium carbonate; In methanol; ethanol; acetic acid;

Reference yield:

: 81502-24-1
3-imino-5-phenyl-9-benzylidene-2,3,6,7,8,9-hexahydro-5H-thiazolo<2,3-b>quinazoline

: 81502-06-9
Sodium; 2-[3-oxo-5-phenyl-9-[1-phenyl-meth-(E)-ylidene]-6,7,8,9-tetrahydro-5H-thiazolo[2,3-b]quinazolin-(2Z)-ylidenemethyl]-benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / conc. HCl / methanol / 12 h / Heating

2: 48 percent / sodium acetate / acetic acid / Heating

With hydrogenchloride; sodium acetate; In methanol; acetic acid;