4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

Base Information

Chemical Name:4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol
CAS No.:80101-83-3
Molecular Formula:C₅₉H₉₂O₄
Molecular Weight:865.377
Hs Code.:

4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

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Chemical Property of 4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

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Technology Process of 4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

There total 4 articles about 4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80101-76-4
Benzoic acid 4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenyl ester

: 80101-83-3,83626-23-7
4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

Guidance literature:: With methanol; potassium hydroxide; at 0 ℃; Yield given;
DOI:10.1246/cl.1982.1131

Reference yield:

: 68799-83-7
Decaprenyl bromide

: 80101-83-3,83626-23-7
4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylsulfoxide; tetrahydrofuran / Ambient temperature

2: 30percent KOH/MeOH / 0 °C

With methanol; potassium hydroxide; sodium hydride; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1246/cl.1982.1131

Reference yield:

: 80101-87-7
4-benzoyloxy-2,3-dimethoxy-5-methylphenol

: 80101-83-3,83626-23-7
4-((2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-Decamethyl-tetraconta-2,6,10,14,18,22,26,30,34,38-decaenyloxy)-2,3-dimethoxy-6-methyl-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylsulfoxide; tetrahydrofuran / Ambient temperature

2: 30percent KOH/MeOH / 0 °C

With methanol; potassium hydroxide; sodium hydride; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1246/cl.1982.1131