Technology Process of C23H33NO6
There total 9 articles about C23H33NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: diisobutylaluminium hydride / dichloromethane / -78 °C
2: pyridine
3: pyridinium p-toluenesulfonate / ethanol
4: pyridinium dichromate / dichloromethane / Molecular sieve
5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol
6: triethylamine; dicyclohexyl-carbodiimide / dichloromethane
7: ammonium formate; triethylamine / 1,4-dioxane
8: 1,2-dichloro-ethane / Reflux
9: 0 °C
With
pyridine; sodium chlorite; pyridinium dichromate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; ammonium formate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; triethylamine; dicyclohexyl-carbodiimide;
In
1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1055/s-0030-1260812
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridinium p-toluenesulfonate / ethanol
2: pyridinium dichromate / dichloromethane / Molecular sieve
3: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol
4: triethylamine; dicyclohexyl-carbodiimide / dichloromethane
5: ammonium formate; triethylamine / 1,4-dioxane
6: 1,2-dichloro-ethane / Reflux
7: 0 °C
With
sodium chlorite; pyridinium dichromate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; ammonium formate; pyridinium p-toluenesulfonate; triethylamine; dicyclohexyl-carbodiimide;
In
1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1055/s-0030-1260812
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium dichromate / dichloromethane / Molecular sieve
2: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol
3: triethylamine; dicyclohexyl-carbodiimide / dichloromethane
4: ammonium formate; triethylamine / 1,4-dioxane
5: 1,2-dichloro-ethane / Reflux
6: 0 °C
With
sodium chlorite; pyridinium dichromate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; ammonium formate; triethylamine; dicyclohexyl-carbodiimide;
In
1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1055/s-0030-1260812