Calix[4]resorcinarene

Base Information

• Chemical Name: Calix[4]resorcinarene
• CAS No.: 260786-76-3
• Molecular Formula: C₃₂H₃₂O₈
• Molecular Weight: 544.601
• Mol file: 260786-76-3.mol

Synonyms:

Chemical Property of Calix[4]resorcinarene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Calix[4]resorcinarene

There total 2 articles about Calix[4]resorcinarene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C72H24(2)H72O24 (1335371-17-9) → isobutene-d8 (20762-54-3) + Calix[4]resorcinarene (260786-76-3,789483-67-6,443770-31-8)

Guidance literature:

With triphenylsulfonium nonafluoro-n-butanesulfonate; at 80 ℃; for 0.0166667h; Film; UV-irradiation;

DOI:10.1071/CH11242

Reference yield:

paracetaldehyde (123-63-7) + recorcinol (108-46-3) → Calix[4]resorcinarene (260786-76-3,789483-67-6,443770-31-8) + 4,4'-(ethane-1,1-diyl)bis(benzene-1,3-diol) (432041-90-2) + 4-[(S)-1-(2,4-Dihydroxy-phenyl)-ethyl]-6-[(R)-1-(2,4-dihydroxy-phenyl)-ethyl]-benzene-1,3-diol (134938-95-7) + 4,6-Bis-[(R)-1-(2,4-dihydroxy-phenyl)-ethyl]-benzene-1,3-diol (134938-96-8)

Guidance literature:

With hydrogenchloride; d⁽⁴⁾-methanol; In 1,4-dioxane; at 26.9 ℃; for 22h; Rate constant; Mechanism; other conditions: other times, other solvent;

DOI:10.1021/jo00019a011

Reference yield: 97.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (S)-1-phenyl-ethylamine (2627-86-3) + Calix[4]resorcinarene (260786-76-3,789483-67-6,443770-31-8) → r2,c8,c14,c20-Tetramethyl-5,11,17,23-tetrakis<<(S)-1-phenylethylamino>methyl>pentacyclo<19.3.1.13,7.19,13.115,19> octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaen-4,6,10,12,16,18,22,24-octol

Guidance literature:

In ethanol; benzene; at 20 ℃; for 24h;

DOI:10.1023/A:1012346126678

upstream raw materials:

paracetaldehyde

recorcinol

C₇₂H₂₄⁽²⁾H₇₂O₂₄

Downstream raw materials:

4,6,10,12,16,18,22,24-Octakis(benzoyloxy)-2,8,14,20-tetramethylpentacyclo<19.3.1.1^3,7.1^9,13.1^15,19>octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaen

C₆₄H₆₀N₄O₈

C₁₂₈H₁₀₄O₃₂P₈

C₆₈H₇₂O₁₆S₄