meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate

Base Information

Chemical Name:meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate
CAS No.:77029-23-3
Molecular Formula:C₂H₃N*C₄₀H₄₀As₄Ni*2F₆P
Molecular Weight:1210.11
Hs Code.:

meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate

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Chemical Property of meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate

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Technology Process of meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate

There total 1 articles about meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: ammonium hexafluorophosphate

: racemic-o-phenylenebis(methylphenylarsine)

: 6018-89-9
nickel(II) acetate tetrahydrate

: 75-05-8,26809-02-9
acetonitrile

: 77029-23-3
meso-((RR)-o-phenylenebis(methylphenylarsine))((SS)-o-phenylenebis(methylphenylarsine))nickel(II) hexafluorophosphate acetonitrile solvate

Guidance literature:: In ethanol; acetonitrile; suspn. nickel(II) acetate, (RR,SS)-diars and NH4PF6 in ethanol heated under reflux with stirring for 15 min, react. mixt. evapd., residue heated in vacuo (100°C, 20 mmHg), solid washed with water, dried and crystd. from acetonitrile; elem. anal.;