trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

Base Information

Chemical Name:trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]
CAS No.:252659-37-3
Molecular Formula:C₅₃H₄₉FeNP₄
Molecular Weight:879.721
Hs Code.:

trans-[FeH(CN)(PPh<sub>2</sub>(CH<sub>2</sub>)2PPh<sub>2</sub>)2]

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Chemical Property of trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

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Technology Process of trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

There total 9 articles about trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: potassium cyanide

: 252659-29-3
trans-[FeH(3-methoxypropionitrile)(dppe)2][BF₄]

: 252659-37-3,67827-23-0,70428-49-8
trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

Guidance literature:: In tetrahydrofuran; methanol; Ar-atmosphere; slight excess of KCN, stirring in THF/MeOH=1:1 for 12 h; solvent removal (vac.), extn. with CH2Cl2, washing (hexane);
DOI:10.1016/S0022-328X(99)00392-7

Reference yield: 89.0%

: potassium cyanide

: 19392-93-9,32490-70-3
trans-hydridochloro-di-{1,2-bis(diphenylphosphino)ethane}iron(II)

: 252659-37-3,67827-23-0,70428-49-8
trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

Guidance literature:: In tetrahydrofuran; methanol; a soln. of KCN (2.3 mmol) in MeOH was added to a soln. of trans-Fe-contg. compd. (1.1 mmol) in THF; stirring for 1 h under Ar; the solvent was removed; extd. into toluene; removal of the toluene; elem. anal.;
DOI:10.1039/b0056871

Reference yield: 88.0%

: 773837-37-9
sodium cyanide

: 38831-81-1
trans-{FeH(NCCH₃)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2}B(C₆H₅)4

: 252659-37-3,67827-23-0,70428-49-8
trans-[FeH(CN)(PPh₂(CH₂)2PPh₂)2]

Guidance literature:: In tetrahydrofuran; methanol; Ar-atmosphere; slight excess of NaCN, stirring in THF/MeOH=1:1 for 8 h; solvent removal (vac.), extn. with CH2Cl2, washing (hexane); elem. anal.;
DOI:10.1016/S0022-328X(99)00392-7